Tanaka R, Kawamura M, Mizutani S, Kikura-Hanajiri R (2023) Identification of LSD analogs, 1cP-AL-LAD, 1cP-MIPLA, 1V-LSD and LSZ in sheet products. Part VI: Analytical and behavioural characterization of 1-cyclopropanoyl- d-lysergic acid diethylamide (1CP-LSD). īrandt SD, Kavanagh PV, Westphal F, Stratford A, Odland AU, Klein AK, Dowling G, Dempster NM, Wallach J, Passie T, Halberstadt AL (2020) Return of the lysergamides. Part V: analytical and behavioural characterization of 1-butanoyl- d-lysergic acid diethylamide (1B-LSD). īrandt SD, Kavanagh PV, Westphal F, Stratford A, Elliott SP, Dowling G, Wallach J, Halberstadt AL (2019) Return of the lysergamides. Tanaka R, Kawamura M, Hakamatsuka T, Kikura-Hanajiri R (2020) Identification of LSD derivatives, 1cP-LSD, MIPLA and 1B-LSD in illegal products as paper sheet. Part I: analytical and behavioural characterization of 1-propionyl- d -lysergic acid diethylamide (1P-LSD).
īrandt SD, Kavanagh PV, Westphal F, Stratford A, Elliott SP, Hoang K, Wallach J, Halberstadt AL (2016) Return of the lysergamides. Tanaka R, Kawamura M, Hakamatsuka T, Kikura-Hanajiri R (2020) Identification and analysis of LSD derivatives in illegal products as paper sheet. Mitteilung über Mutterkornalkaloide Helv Chim Acta 40:1706–1720. Troxler F, Hofmann A (1957) Substitutionen am ringsystem der lysergsäure I. EMCDDA-Europol 2015 Annual Report on the implementation of Council Decision 2005/387/JHA. European Monitoring Centre for Drugs and Drug Addiction (EMCDDA). Stoll A, Hofmann A (1943) Partialsynthese von alkaloiden vom typus des ergobasins. This type of lysergamide may become prevalent in the near future, and we should remain alert for newly appearing lysergamides. To the authors’ knowledge, this is the first case report in which 1-(thiophene-2-carbonyl)-LSD was seized and the first seizure of an LSD analog in which an aromatic carboxylic acid had been condensed to LSD. ConclusionĪs in this case, similar blotter paper analyses should consider the possibility of a mismatch between the label and ingredient. Instrumental analyses confirmed the active compound to be 1-(thiophene-2-carbonyl)-LSD, which was inconsistent with the labeling on drug-infused blotter paper. The contents of the seized specimens were identified using authentic standard analysis with GC/MS, LC/MS, and NMR spectroscopy. The estimated compound was then synthesized, yielding an authentic standard. One of the seized specimens was extracted and analyzed using gas chromatography/mass spectrometry (GC/MS), liquid chromatography/mass spectrometry (LC/MS), high-resolution mass spectrometry (HRMS), and nuclear magnetic resonance (NMR) spectroscopy to estimate the extract components. Herein, we determined the structure of the absorbed compound. Because this analog is much more difficult to synthesize than previously reported LSD analogs, we doubted that the blotter paper contained 1D-LSD. Several websites indicate that 1D-LSD is 1-(1,2-dimethylcyclobutane-1-carbonyl)-LSD.
In this case, three pieces of blotter paper labeled “1D-LSD” and presumably impregnated with this LSD analog, were seized. Since the mid-2010s, lysergic acid diethylamide (LSD) analogs made for substance abuse have periodically emerged.
0 kommentar(er)
